Caution: JavaScript execution is disabled in your browser or for this website. You may not be able to answer all questions in this survey. Please, verify your browser parameters.

ACTNXT survey

To reach its climate neutrality goals Europe needs to rely heavily on Power-to-X (PtX) technology to replace the many applications of fossil fuels that are not easily electrified. Many PtX technologies are however still immature or not ready for deployments yet, highlighting the need for a sustained R&D effort in the field.

Neutron- and synchrotron sources can play a crucial role in this effort, however lack of key instrumentation is limiting the current possibilities.

ACTNXT will upgrade the instrumentation at current neutron- and synchrotron sources to enable it to provide crucial knowledge within PtX areas such as efficiency, safety, price, raw material consumption, and durability. This will be done by developing instrumentation for:

1. Operando measurements of processes and flow inside PtX components

2. Materials behaviour under hydrogen exposure

3. Reliable and high throughput investigation of novel materials

4. Operando measurements of hazardous chemical reactions

The new instrumentation will be designed for broad adaptation as upgrades for many existing research instruments across Europe. Prototypes of all 4 instrumentation types will be constructed at leading research infrastructures and their capabilities tested and demonstrated. This is supplemented by a common knowledge platform addressing common challenges such as safety and planning of complicated experiments.

During the project, the consortium will have a very strong dialogue with the user communities to ensure that the developed instrumentation matches its needs and that it is ready to take full advantage of the instrumentation also after the end of the project. In doing so ACTNXT aims to give the European green industry a huge boost and ensure that it captures a major part of an emerging trillion Euro PtX market.

Thank you for participating in this survey. The purpose of the following questions is to ensure that the instrumentation developed in ACTNXT will have the maximum impact on the PtX community.

This data will be used only for the purpose of gathering information for the ACTNXT project and will be erased after that.

To proceed, we kindly ask you to check the box below. For more details see our privacy policy.

Introduction
(This question is mandatory)
A0. What PtX topics are you interested in? (Pick as many as you want)
Electrolysis and/or Fuel cells
(This question is mandatory)
B1: Please indicate here your main fields of activity in terms of technology in electrolysis and/or fuel cells. 
(This question is mandatory)
B2.0: You are interested in...
(This question is mandatory)
B2: Field of Electrolyzers : According to you, what are the key/biggest challenges/topics under current development or scale-up that are NOT addressable with existing lab analysis and yet would merit further investigation at a large scale facility/beamline?
Physical structure of the membrane
Physical structure (morphology) of the anode
Physical structure (morphology) of the cathode
Chemical structure of the membrane
Chemical structure of the electrode/coating/catalyst
Liquid / Gas flow analysis
Phase changes or quantitative phase analysis
Materials incorporation in the MEA
Mass transport
Complex phenomena at cell level
Ageing
Physical or chemical characterisation of bipolar plates and/or sealant
Interest in study at stack level
Other
B2bis: Field of Fuel cells: According to you, what are the key/biggest challenges/topics under current development or scale-up that are NOT addressable with existing lab analysis and yet would merit further investigation at a large scale facility/beamline?
Physical structure of the membrane
Physical structure (morphology) of the anode
Physical structure (morphology) of the cathode
Chemical structure of the membrane
Chemical structure of the electrode/coating/catalyst
Liquid / Gas flow analysis
Phase changes or quantitative phase analysis
Materials incorporation in the MEA
Mass transport
Complex phenomena at cell level
Ageing
Physical or chemical characterisation of bipolar plates and/or sealant
Interest in study at stack level
Other
B2.1: If you answered “Phase changes or quantitative phase analysis”, please specify if your comment concerns Electrolyzers or Fuel cells:
B2.2: If you answered “Liquid/Gas flow analysis”, please specify if your comment concerns Electrolyzers or Fuel cells:
B2.3: If you answered “Other”, please specify:
(This question is mandatory)

B3: What are the most strategic aspects in your line of R & D that would need to be investigated? 

Ohmic losses
Catalyst kinetic performance and/or PGM thrifting
High pressure operation
Mass transport
Gas Cross over
Membrane research
Long term durability
Transient phenomena
Component performance
Sensitivity of various manufacturing parameters
System engineering
Other
(This question is mandatory)
B3.1: If you answered “Sensitivity of various manufacturing parameters”, please specify:
(This question is mandatory)
B3.2: If you answered “Other”, please specify:
(This question is mandatory)
B3bis: What kinds of electrochemical characterisations would be needed?
(This question is mandatory)
B4: What component (or material) would you like to be studied)?
Flow field
Membrane
Ionomer
Anode catalyst
Cathode catalyst
Diaphragm (separator)
Porous transport electrode (PTE)
Membrane Electrode Assembly (MEA)
Single cell
Full Stack
GDL
Other (e.g. sealants)
(This question is mandatory)
B4.1: If you answered “Other”, please specify:
(This question is mandatory)
B5: Which operating parameters are important for you to consider during the study?
Temperature
Pressure
Flow rate
Humidity
(High) current density
Voltage
Contaminants
Active area
Other
(This question is mandatory)
B5.2: If you answered 1-5 to “Pressure”, please indicate a desired range [bar (anode/cathode)]:
(This question is mandatory)
B5.1: If you answered 1-5 to “Temperature”, please indicate a desired range [°C ]:
(This question is mandatory)
B5.3: If you answered 1-5 to “Flow rate (specify units)”, please indicate a desired range and liquid composition:
(This question is mandatory)
B5.4: If you answered 1-5 to “(High) current density”, please specify desired current:
(This question is mandatory)
B5.5: If you answered 1-5 to “Contaminants”, please specify contaminants:
(This question is mandatory)
B5.6: If you answered 1-5 to “Active area”, please indicate a desired size cm2:
(This question is mandatory)
B5.7: If you answered “Other”, please specify:
(This question is mandatory)
B6: Please indicate the preferred workflows that would best fit your R & D needs:
B6.1: If you answered "Operando", please specify the relevant time scale (minutes, days, weeks...):
(This question is mandatory)
B7.1: Typical techniques required for your R & D needs. Please indicate type of probe needed:
(This question is mandatory)
B7.2: Typical techniques required for your R & D needs. Please indicate characterisation category and where possible the specific technique needed:
(This question is mandatory)
B7.3: Typical techniques required for your R & D needs. Please indicate characteristic length and/or time scale:
B7.4: Additional comments you may have about typical characterisation techniques and probes:
(This question is mandatory)
B8: What is the main/most pressing experiment/characterisation that you think needs to be carried out to push hydrogen technology further?
Materials under exposure to hydrogen or other gases
(This question is mandatory)
C1: What gases (or liquids) are you most interested in?
H2
Liquid H2
NH3
Liquid NH3
Hydrocarbons
Other
(This question is mandatory)
C1.1: If you answered 1-5 to "Other", please specify what gases or liquids you are interested in:
(This question is mandatory)
C2.1: Please specify how important the following type of information is to you?
2D structural mapping
3D structural mapping
Crack initiation
Crack propagation
Bubble / Imperfection sizes
Time-resolved measurements
Stresses
Metallic phases
Surface chemistry
Hydrogen mobility
Texture
Hydrogen depth profile
Other information
C2.2: If you answered that you found the above information important, please specify the resolution you would require:
2D structural mapping
3D structural mapping
Crack propagation
Bubble sizes
(This question is mandatory)
C2.3: If you answered 1-5 to “Other information” please specify what information and indicate a size scale if relevant:
(This question is mandatory)
C3: What environment(s) would you like to expose your sample(s) to during or immediately before measurements?
Pressure
Temperature
Forces
Fatigue testing
Knowledge of impurities in the gases
Control of impurities in the gases
Others
(This question is mandatory)
C3.1:If you answered 1-5 to “Pressure”, please indicate a desired range:
(This question is mandatory)
C3.2: If you answered 1-5 to “Temperature”, please indicate a desired range:
(This question is mandatory)
C3.3: If you answered 1-5 to “Forces”, please indicate a desired range and type (e.g. compressive, torque,…):
(This question is mandatory)
C3.4: If you answered 1-5 to “Others” please specify what environments:
(This question is mandatory)
C3.5: If you answered yes to "knowledge of impurities" or "control of impurities" in the gases please specify which:
Humidity
Sulfur
CO2
02
Other
(This question is mandatory)
C3.5.1: If you answered “Knowledge is important" to “Other” please specify:
(This question is mandatory)

C4: What materials are you interested in investigating?

Al
Steel
Ti
Cu
Ni-based alloys
Plastics
Composites
Membranes
Electrodes
Materials for hydrogen storage (e.g., MOFs)
Coatings
Others
(This question is mandatory)
C4.1: If you answered 1-5 to “Coatings” please specify the materials and thicknesses you are interested in:
(This question is mandatory)
C4.2: If you answered 1-5 to “Others” please specify:
(This question is mandatory)

C5: Finally, if you have other comments for Materials under exposure to hydrogen and other gases, please add them below:

Chemical conversion (e.g., in catalyst materials or electrolytes)
(This question is mandatory)
D1: What (if any) types of information would you like to be able to measure while keeping your samples in a protected atmosphere (e.g., in a glove box)?
2D structure
3D structure
Time development
Material composition
Surface chemistry
Impurity mapping
Sample degradation
Crack initiation
Crack propagation
Stress / Strain
Others
(This question is mandatory)
D1.1: If you answered 1-5 to “2D structure” please specify the resolution you are interested in:
(This question is mandatory)
D1.2: If you answered 1-5 to “3D structure” please specify the resolution you are interested in:
(This question is mandatory)
D1.3: If you answered 1-5 to “Time development” please specify the resolution you are interested in:
(This question is mandatory)
D1.4: If you answered 1-5 to “Sample degradation” please specify the processes you are interested in:
(This question is mandatory)

D2: What types of samples would you be interested in analyzing in a protective atmosphere?

Electrodes
Catalyst materials
Materials for hydrogen storage (e.g., MOFs)
Battery electrolytes
Samples associated with safety concerns (e.g. toxic / combustible samples)
Other samples
(This question is mandatory)
D2.1: If you answered 1-5 to “Catalyst materials” please specify the materials you are interested in:
(This question is mandatory)
D2.2: If you answered 1-5 to “Samples associated with safety concerns” please specify:
(This question is mandatory)
D3: What inert gas would you like to be provided in the glove box?
(This question is mandatory)

D4: Would you be interested in the utilization of an in-line glovebox for (operando) neutron imaging experiments?

In case you would like to know more about neutron imaging and its broad range of applications, please visit the following websites (What is Neutron Imaging ? | Applied Materials | PSI) (Research at Applied Materials Group | Applied Materials | PSI). Alternatively, more detailed information about the state-of-the-art neutron imaging can be found in the recently published book (Neutron Imaging - Book - IOPscience). 

D5: What other specific features should the glove box be equipped with? Please detail your wishes below:

Other Areas of Interest
(This question is mandatory)

OAI1. Please specify areas that you may be interested in, under what conditions and what questions you would like to explore.

Examples:

  • “Area of interest: Hydrogen Storage.”
  • “Parameters of interest: 4-300 K, 1-100 bar.”
  • “Questions of interest: what happens to the MOF structure during cyclical loading and unloading of hydrogen, Where is the hydrogen located."
About You
YOU0: Finally, here are a few follow up questions to understand better your environment and needs:
(This question is mandatory)
YOU1: What organization(s) are you affiliated with?
(This question is mandatory)

YOU2: What are you mainly working on?

(This question is mandatory)
YOU3. Do you have previous experience with neutron and synchrotron analysis?
(This question is mandatory)
YOU4: Are you interested in supplying samples to test the instrumentation developed through ACTNXT?
(This question is mandatory)
YOU5: Do you authorise us to contact you to elaborate on your answers?
(This question is mandatory)

YOU45: If you answered “Yes” to either being willing to provide samples or elaborate on your answers, please provide one or more ways to contact you.

The ACTNXT consortium will keep the contact information for the remainder of the project unless specifically asked to delete it before.

This information will only be used to elaborate on the questions given above unless otherwise agreed upon:

YOU6: If you have any other comments or inputs, please detail them below:

YOU7: If you are keen to take part in a more technical survey regarding the test benches for users of neutron and synchrotron sources, please copy this link into your browser 

 https://survey.ill.fr/index.php/721171

Do NOT forget to submit this form before completing the other survey.